HCID 13746888, compound → N-(4,5-dihydro-1-ethyl-1H-pyrazol-4-yl)4-nitrobenzamide

HRID 1732035Notes

Reaction equation

[CH2:1]([N:3]1[CH2:7][CH:6]([NH:8][C:9](=[O:19])[C:10]2[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][CH:11]=2)[CH2:5][N:4]1CC)[CH3:2].Cl[O-].[Na+]>>[CH2:1]([N:3]1[CH2:7][CH:6]([NH:8][C:9](=[O:19])[C:10]2[CH:11]=[CH:12][C:13]([N+:16]([O-:18])=[O:17])=[CH:14][CH:15]=2)[CH:5]=[N:4]1)[CH3:2]

Participants

Reactant 2

HCID 13746888HCID 13746888, compound

HCID 23665760Sodium Hypochlorite

Product 1

HCID 20263149N-(4,5-dihydro-1-ethyl-1H-pyrazol-4-yl)4-nitrobenzamide

Procedure

In accordance with the procedure of Example 12, N-(1,2-diethyl-4-pyrazolidinyl)-4-nitrobenzamide is reacted with sodium hypochlorite and the product is isolated.

Workup

customthe product is isolated

Sources & evidence

ORD record: ord-92179f53580240deb1cc2ceb2f20e02c
Source dataset: uspto-grants-1986_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04624961

Reaction notes

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