4-Amino-N-(1,2-diethyl-4-pyrazolidinyl)benzamide → 4-Amino-N-(4,5-dihydro-1-ethyl-1H-pyrazol-4-yl)benzamide

HRID 1732036Notes

Reaction equation

[NH2:1][C:2]1[CH:19]=[CH:18][C:5]([C:6]([NH:8][CH:9]2[CH2:13][N:12](CC)[N:11]([CH2:16][CH3:17])[CH2:10]2)=[O:7])=[CH:4][CH:3]=1.Cl[O-].[Na+]>>[NH2:1][C:2]1[CH:19]=[CH:18][C:5]([C:6]([NH:8][CH:9]2[CH2:10][N:11]([CH2:16][CH3:17])[N:12]=[CH:13]2)=[O:7])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 104004874-Amino-N-(1,2-diethyl-4-pyrazolidinyl)benzamide

HCID 23665760Sodium Hypochlorite

Product 1

HCID 202631484-Amino-N-(4,5-dihydro-1-ethyl-1H-pyrazol-4-yl)benzamide

Procedure

In accordance with the procedure of Example 12, 4-amino-N-(1,2-diethyl-4-pyrazolidinyl)benzamide is reacted with sodium hypochlorite and the product is isolated.

Workup

customthe product is isolated

Sources & evidence

ORD record: ord-e0389c56dda045c79d3a56995914e571
Source dataset: uspto-grants-1986_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04624961

Reaction notes

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