HCID 20263150, compound → HCID 20226456, compound
Reaction equation
[Cl:1][C:2]1[C:3]([N:22]([CH3:24])[CH3:23])=[CH:4][C:5]([O:20][CH3:21])=[C:6]([CH:19]=1)[C:7]([NH:9][CH:10]1[CH2:14][N:13](CC)[N:12]([CH2:17][CH3:18])[CH2:11]1)=[O:8].Cl[O-].[Na+]>>[CH2:17]([N:12]1[CH2:11][CH:10]([NH:9][C:7](=[O:8])[C:6]2[CH:19]=[C:2]([Cl:1])[C:3]([N:22]([CH3:23])[CH3:24])=[CH:4][C:5]=2[O:20][CH3:21])[CH:14]=[N:13]1)[CH3:18]Participants
3
Procedure
In accordance with the procedure of Example 12, 5-chloro-4-(dimethylamino)-2-methoxy-N-(1,2-diethyl-4-pyrazolidinyl) benzamide is reacted with sodium hypochlorite and the product is isolated.
Workup
- customthe product is isolated
Sources & evidence
- ORD record
- ord-256fea0f6f434f318b824c79d502e0e2
- Source dataset
- uspto-grants-1986_11
- Patent number
- US04624961
Reaction notes
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