HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13786411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | 4-(Bromoacetyl)benzonitrile | HCID 98654 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13786411 | HCID 13786411 | — |
Reaction Steps
p-Cyanophenacyl bromide (29.8 g, 0.138 mole) and p-bromoaniline (47.13 g, 0.266 mole) were combined with 53.2 g of absolute ethanol and stirred 16 hours. The solution was then diluted with ether and the resulting slurry filtered. The filter cake was repulped in 500 ml ether, filtered, repulped in 400 ml acetone and again filtered to yield title product: 17.14 g (40.9%); m.p. 154°-157°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04624958 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-72eba4db359d46e8a16b26449fef6d06 |
| Source note | uspto-grants-1986_11 |