HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[(1,2-Dihydro-1-methyl-2-quinolinyl)methoxy]-α-pentylbenzenemethanol → HCID 20226659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[(1,2-Dihydro-1-methyl-2-quinolinyl)methoxy]-α-pentylbenzenemethanol | HCID 20226651 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20226659 | HCID 20226659 | — |
Reaction Steps
A mixture of 0.88 g (0.0025 mol) N-methyl-1,2,-dihydro-2-[3-(1-hydroxyhexyl)phenoxymethyl]quinoline and 0.05 g Pd/C (10%) in 100 ml ethanol was hydrogenated at 50 psi for a period of 2 hours. After filtration and evaporation of the solvent under reduced pressure, the residue was passed through a silica gel column and the desired product was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04625034 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-f71715a77495411ead0442b6d61c6f15 |
| Source note | uspto-grants-1986_11 |