HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 13723407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Bis(2-oxo-3-oxazolidinyl)phosphinic chloride | HCID 152842 | — |
| Reactant | 2-Anilino-4-oxo-4,5-dihydrofuran-3-carboxylic acid | HCID 6919196 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13723407 | HCID 13723407 | — |
Reaction Steps
The title derivative was obtained by a procedure similar to that described in Example 8 starting with 2-anilino-4-oxo-3-furoic acid (7.01 grams, 0.032 mol), triethylamine (8.98 ml, 0.064 mol), BOP-Cl (8.15 grams, 0.032 mol) and aniline (2.95 ml, 0.32 mol) dissolved in 100 ml methylene chloride. Yield: 7.37 g, mp 175°-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04625040 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-57afd67e8883426e9d57e70581247aec |
| Source note | uspto-grants-1986_11 |