HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 13900787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13631041 | HCID 13631041 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 13900787 | HCID 13900787 | 58% |
Reaction Steps
146 mg of (4RS)-4-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline oxalate, 0.06 ml of carbon disulfide, 0.06 ml of methyl iodide, 0.14 ml of triethylamine and 2 ml of dimethylsulfoxide are treated in the same manner as described in Example 17. 85 mg of methyl (4RS)-4-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline-2-carbodithioate are obtained as pale yellow powder. Yield: 58%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04625032 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-31e1813817664528b1e4ba47764461e8 |
| Source note | uspto-grants-1986_11 |