HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → N,N-Dimethylaminopropyl acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-Hydroxypropanamide | HCID 4145140 | — |
| Product | N,N-Dimethylaminopropyl acrylamide | HCID 77452 | — |
Reaction Steps
59.3 g of β-hydroxypropionic acid amide and 68 g of 3-dimethylaminopropylamine were heated for 5 hours in a temperature range of 125°-168° C. until the evolution of ammonia was complete. After adding 1 g of pulverised sodium hydroxide the reaction mixture was distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237067 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-9fb2048b1977420aad17c78493b3ea51 |
| Source note | uspto-grants-1980_12 |