Ammonia → HCID 20305835, compound

HRID 1732228Notes

Reaction equation

HRID 1732228 reaction equation
[CH:1]([O:4][CH2:5][CH2:6][C:7]([NH2:9])=[O:8])([CH3:3])[CH3:2].[CH3:10][N:11]([CH3:16])[CH2:12][CH2:13][CH2:14]N.N>>[CH3:10][N:11]([CH3:16])[CH2:12][CH2:13][CH2:14][NH:9][C:7](=[O:8])[CH2:6][CH2:5][O:4][CH:1]([CH3:3])[CH3:2]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 7993N,N-Dimethyl-1,3-propanediamineHCID 22238943HCID 22238943, compound

Product 1

HCID 20305835HCID 20305835, compound

Procedure

131.2 g (1.0 mole) of 3-isopropoxypropionamide are heated with 1.07.3 g (1.05 mole) of 3-dimethylaminopropylamine for 6 hours in a temperature range of 145°-170° C. until the evolution of ammonia is complete. In the subsequent distillation in a high vacuum 198 g (0.92 mole=91.5% of the theoretical yield) of colorless liquid are obtained having a Bp0.1 of 128°-132° C.

Workup

  1. distillationIn the subsequent distillation in a high vacuum 198 g (0.92 mole=91.5% of the
  2. customtheoretical yield) of colorless liquid
  3. customare obtained
  4. customa Bp0.1 of 128°-132° C.

Sources & evidence

ORD record
ord-4b484c02693147e49043cb697861e94a
Source dataset
uspto-grants-1980_12
Patent number
US04237067

Reaction notes

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