HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 12546902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 12546817 | HCID 12546817 | — |
| Reactant | HCID 12546900 | HCID 12546900 | — |
| Reactant | Sodium Acetate Trihydrate | HCID 23665404 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12546902 | HCID 12546902 | 93% |
Reaction Steps
This compound was prepared analogously to 3-bromo-2'-ethyl-6'-methylpropionanilide of Example 11A from 20 g 4-propoxy-2,6-xylidine, 95 ml glacial acetic acid, 37 g sodium acetate trihydrate, 150 ml water 21.2 g 3-bromopropionyl bromide. The yield was 93% of recrystallized (methanol:water) material melting at 121.5°-122.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237068 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-291e90b1b55747cea9dc4789ebc1ca86 |
| Source note | uspto-grants-1980_12 |