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HRID1732290

反应详情

EQUATION

反应方程式

HRID 1732290 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(ON=C(C(=O)O)c1csc(N)n1)C(=O)OC(c1ccccc1)c1ccccc1.Cl
HCID89885005

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(ON=C(C(=O)O)c1csc(N)n1)C(=O)OC(c1ccccc1)c1ccccc1
HCID53674735

2-Amino-α-[[2-(diphenylmethoxy)-1,1-dimethyl-2-oxoethoxy]imino]-4-thiazoleacetic acid

C22H21N3O5S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A suspension of the hydrochloride salt product from part (e) in water (20 ml./g.) is adjusted to pH 2.6 and stirred for 30 minutes at 0°. The resulting suspension is filtered, washed thoroughly with water, and dried to yield 2-(2-amino-4-thiazolyl)-2-(1-diphenylmethoxycarbonyl-1-methylethoxy)iminoacetic acid.

WORKUP

后处理

  1. filtrationThe resulting suspension is filtered
  2. washwashed thoroughly with water
  3. customdried