HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 131711959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Reactant | HCID 131711960 | HCID 131711960 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131711959 | HCID 131711959 | — |
Reaction Steps
10.0 g of dimethylphenylsilylmethyl acetoacetate, 3.0 g of 3-nitrobenzaldehyde and 2.2 ml of concentrated ammonia in 15 ml of 96 percent strength ethanol are heated under reflux for 20 hours. After cooling and filtering, 11.0 g of yellow crystals of melting point 125° C. (ethanol) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237137 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-f298efc33d5a45ba84061d0814ec4405 |
| Source note | uspto-grants-1980_12 |