HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 13081186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Reactant | HCID 11481114 | HCID 11481114 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13081186 | HCID 13081186 | — |
Reaction Steps
After boiling 5.0 g of 2-trimethylsilylethyl acetoacetate, 1.9 g of 3-nitrobenzaldehyde and 1.5 ml of concentrated ammonia in 10 ml of 96 percent strength ethanol for 20 hours, then cooling and filtering off the product, 3.5 g of pale yellow crystals of melting point 120° C. (ethanol) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237137 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-5d6c9158f2da4cff9cc91fd86eebbd39 |
| Source note | uspto-grants-1980_12 |