3-Chloro-2-methyl-1-propene → HCID 14022403, compound

HRID 1732334Notes

Reaction equation

HRID 1732334 reaction equation
[C:1]([N:4]1[CH2:9][CH2:8][CH:7]([OH:10])[CH2:6][CH2:5]1)(=[O:3])[CH3:2].[CH3:11][C:12](=[CH2:15])[CH2:13]Cl>>[C:1]([N:4]1[CH2:9][CH2:8][CH:7]([O:10][CH2:13][C:12]([CH3:15])=[CH2:11])[CH2:6][CH2:5]1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 112413-Chloro-2-methyl-1-propeneHCID 107492911-(4-Hydroxypiperidin-1-yl)ethan-1-one

Product 1

HCID 14022403HCID 14022403, compound

Procedure

This compound was prepared similarly to Example E, starting from N-acetyl-4-hydroxypiperidine and 2-methylallyl chloride, and was distilled and used directly in the next stage. It had a b.p. of 128° C. @ 1 mm.

Workup

  1. customThis compound was prepared similarly to Example E
  2. distillationwas distilled

Sources & evidence

ORD record
ord-9c540647bda44c769d6c744d0454a484
Source dataset
uspto-grants-1980_12
Patent number
US04237138

Reaction notes

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