L 636499 → HCID 9882008, compound

HRID 1732353Notes

Reaction equation

HRID 1732353 reaction equation
[CH:1]1[C:11]2[CH2:10][CH2:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[S:6](=[O:17])(=[O:16])[C:5]=2[CH:4]=[C:3]([C:18](O)=[O:19])[CH:2]=1.C1C2C=CC3C=CC=CC=3S(=O)(=O)C=2C=C(C(O)=O)C=1>>[OH:19][CH2:18][C:3]1[CH:2]=[CH:1][C:11]2[CH2:10][CH2:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[S:6](=[O:17])(=[O:16])[C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 130562L 636499HCID 9795947HCID 9795947, compound

Product 1

HCID 9882008HCID 9882008, compound

Procedure

Repeat the process of Example 6, substituting an equivalent quantity of 10,11-dihydrodibenzo[b,f]thiepin-3-carboxylic acid-5,5-dioxide for the dibenzo[b,f]thiepin-3-carboxylic acid-5,5-dioxide, to obtain the title product (m.p., 128°-130° C.).

Sources & evidence

ORD record
ord-f09ed6a0aabf423084455d7a6d3afc68
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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