L 636499 → HCID 20306156, compound

HRID 1732366Notes

Reaction equation

HRID 1732366 reaction equation
[SH:1][C:2]1[CH:3]=[CH:4][C:5]2[S:11](=[O:13])(=[O:12])[C:10]3[CH:14]=[C:15]([C:18](O)=[O:19])[CH:16]=[CH:17][C:9]=3[CH2:8][CH2:7][C:6]=2[CH:21]=1.C1C2C=CC3C=CC=CC=3S(=O)(=O)C=2C=C(C(O)=O)C=1>>[OH:19][CH2:18][C:15]1[CH:16]=[CH:17][C:9]2[CH2:8][CH2:7][C:6]3[CH:21]=[C:2]([SH:1])[CH:3]=[CH:4][C:5]=3[S:11](=[O:13])(=[O:12])[C:10]=2[CH:14]=1

Participants

3

Reactant 2

HCID 130562L 636499HCID 54372008HCID 54372008, compound

Product 1

HCID 20306156HCID 20306156, compound

Procedure

Repeat the process of Example 6, substituting an equivalent quantity of 8-mercapto-10,11-dihydrodibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide for the dibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide, to obtain the title product.

Sources & evidence

ORD record
ord-3fe0107bc326436486698aa44de647e4
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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