L 636499 → HCID 20306162, compound

HRID 1732370Notes

Reaction equation

HRID 1732370 reaction equation
[CH3:1][S:2][C:3]1[CH:4]=[CH:5][C:6]2[S:12](=[O:14])(=[O:13])[C:11]3[CH:15]=[C:16]([C:19](O)=[O:20])[CH:17]=[CH:18][C:10]=3[CH:9]=[CH:8][C:7]=2[CH:22]=1.C1C2C=CC3C=CC=CC=3S(=O)(=O)C=2C=C(C(O)=O)C=1>>[OH:20][CH2:19][C:16]1[CH:17]=[CH:18][C:10]2[CH:9]=[CH:8][C:7]3[CH:22]=[C:3]([S:2][CH3:1])[CH:4]=[CH:5][C:6]=3[S:12](=[O:14])(=[O:13])[C:11]=2[CH:15]=1

Participants

3

Reactant 2

HCID 130562L 636499HCID 20271497HCID 20271497, compound

Product 1

HCID 20306162HCID 20306162, compound

Procedure

Repeat the process of Example 6, substituting an equivalent quantity of 8-methylthiodibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide for the dibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide, to obtain the title product.

Sources & evidence

ORD record
ord-f77ba81d20c44ef98e58fa59e91949e9
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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