L 636499 → HCID 20306173, compound

HRID 1732372Notes

Reaction equation

HRID 1732372 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[CH:7][C:8]2[S:14](=[O:16])(=[O:15])[C:13]3[CH:17]=[C:18]([C:21](O)=[O:22])[CH:19]=[CH:20][C:12]=3[CH:11]=[CH:10][C:9]=2[CH:24]=1)(=[O:4])=[O:3].C1C2C=CC3C=CC=CC=3S(=O)(=O)C=2C=C(C(O)=O)C=1>>[OH:22][CH2:21][C:18]1[CH:19]=[CH:20][C:12]2[CH:11]=[CH:10][C:9]3[CH:24]=[C:5]([S:2]([CH3:1])(=[O:3])=[O:4])[CH:6]=[CH:7][C:8]=3[S:14](=[O:16])(=[O:15])[C:13]=2[CH:17]=1

Participants

3

Reactant 2

HCID 130562L 636499HCID 541059618-Methylsulfonyldibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide

Product 1

HCID 20306173HCID 20306173, compound

Procedure

Repeat the process of Example 6, substituting an equivalent quantity of 8-methylsulfonyldibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide for the dibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide, to obtain the title product.

Sources & evidence

ORD record
ord-5088ffc9e4424d968d09f17d12770489
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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