HCID 13151858, compound → HCID 20306170, compound

HRID 1732375Notes

Reaction equation

HRID 1732375 reaction equation
[OH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[S:12][C:11]3[CH:13]=[C:14]([C:17](O)=[O:18])[CH:15]=[CH:16][C:10]=3[CH2:9][CH2:8][C:7]=2[CH:20]=1.C1C2CCC3C=CC=CC=3SC=2C=C(C(O)=O)C=1>>[OH:18][CH2:17][C:14]1[CH:15]=[CH:16][C:10]2[CH2:9][CH2:8][C:7]3[CH:20]=[C:3]([CH2:2][OH:1])[CH:4]=[CH:5][C:6]=3[S:12][C:11]=2[CH:13]=1

Participants

3

Reactant 2

HCID 13151858HCID 13151858, compoundHCID 20306165HCID 20306165, compound

Product 1

HCID 20306170HCID 20306170, compound

Procedure

Repeat the process of Example 1, substituting an equivalent quantity of 8-hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepin-3-carboxylic acid for the 10,11-dihydrodibenzo[b,f]thiepin-3-carboxylic acid, to obtain the title product.

Sources & evidence

ORD record
ord-43a98baddf024fc8a537b392a3a4d88e
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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