L 636499 → HCID 20255503, compound

HRID 1732383Notes

Reaction equation

HRID 1732383 reaction equation
[F:1][C:2]1[CH:3]=[CH:4][C:5]2[S:11](=[O:13])(=[O:12])[C:10]3[CH:14]=[C:15]([C:18](O)=[O:19])[CH:16]=[CH:17][C:9]=3[CH:8]=[CH:7][C:6]=2[CH:21]=1.C1C2C=CC3C=CC=CC=3S(=O)(=O)C=2C=C(C(O)=O)C=1>>[F:1][C:2]1[CH:3]=[CH:4][C:5]2[S:11](=[O:12])(=[O:13])[C:10]3[CH:14]=[C:15]([CH2:18][OH:19])[CH:16]=[CH:17][C:9]=3[CH:8]=[CH:7][C:6]=2[CH:21]=1

Participants

3

Reactant 2

HCID 130562L 636499HCID 13490390HCID 13490390, compound

Product 1

HCID 20255503HCID 20255503, compound

Procedure

Repeat the process of Example 6, substituting an equivalent quantity of 8-fluorodibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide for the dibenzo[b,f]thiepin-3-carboxylic acid 5,5-dioxide, to obtain the title product (m.p., 131°-133° C.).

Sources & evidence

ORD record
ord-adbcae45ef7b477ca11718db2ae5bb36
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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