HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]- → HCID 70588101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]- | HCID 3006852 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 70588101 | HCID 70588101 | — |
Reaction Steps
In 30.0 g (0.101 mole) of 1-[β-(2,4-dichlorophenyl)hexyl]imidazole dissolved in 200 ml of ether is bubbled dry hydrogen chloride gas until the mixture is acidic to litmus. A colorless solid forms which is separated by filtration to give 24.5 g. of the hydrochloride salt which is identified by nmr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237158 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-abc6ab19c5284c13aa60aff6343797e6 |
| Source note | uspto-grants-1980_12 |