Nitric Acid → HCID 20306119, compound

Participants

Reaction Steps

To a solution of 40 ml of nitric acid and 10 ml of sulfuric acid, 14.8 g (0.0498 mole) of 1-[β-(2,4-dichlorophenyl)hexyl]imidazole in 30 ml of sulfuric acid is added at less than 5°. The reaction is stirred for 1/2 hour and then it is poured into acid water. The oily solid which separates is isolated by decanting off the dilute acid solution. The residue is washed and then treated with ammonium hydroxide solution.

Provenance & Evidence