HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl iodide → HCID 86735891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | 1H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]- | HCID 3006852 | — |
| Product | HCID 86735891 | HCID 86735891 | 66% |
Reaction Steps
1-[β-(2,4-dichlorophenyl)hexyl]imidazole 5.0 g (0.0168 moles) is heated for two hours on a steambath with 3.1 g (0.0168 moles) of 1-iodobutane. The reaction is cooled and triturated three times with 50 ml of ether. The oil residue is stripped to dryness to give 5.3 g (66%) of the oil product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237158 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-93db46822af54007a43325f15d7cd226 |
| Source note | uspto-grants-1980_12 |