Thenyl mercaptan → Ethyl-thenyl-disulphide

HRID 1732417Notes

Reaction equation

[C:1]1([CH2:6][SH:7])[S:5][CH:4]=[CH:3][CH:2]=1.C(N1C(=O)C2=CC=CC=[C:12]2[C:11]1=[S:20])C>>[CH2:11]([S:20][S:7][CH2:6][C:1]1[S:5][CH:4]=[CH:3][CH:2]=1)[CH3:12]

Participants

Reactant 2

HCID 80408Thenyl mercaptan

HCID 57251189N-ethylthiophthalimide

Product 1

HCID 20306424Ethyl-thenyl-disulphide

Procedure

Starting from thenylmercaptan and N-ethylthiophthalimide there is obtained ethyl-thenyl-disulphide. nD20 =1.6044. IR (liq.): bands inter alia at 3000, 1450, 1250, 1035, 850, 700 cm-1 ;

Sources & evidence

ORD record: ord-ca8085ec89cf463a9436eaf28565249c
Source dataset: uspto-grants-1980_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04237290

Reaction notes

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