Thenyl mercaptan → Propyl-thenyl-disulphide

HRID 1732418Notes

Reaction equation

[C:1]1([CH2:6][SH:7])[S:5][CH:4]=[CH:3][CH:2]=1.C(N1C(=O)C2=CC=C[CH:20]=[C:13]2[C:12]1=[S:21])CC>>[CH2:12]([S:21][S:7][CH2:6][C:1]1[S:5][CH:4]=[CH:3][CH:2]=1)[CH2:13][CH3:20]

Participants

Reactant 2

HCID 80408Thenyl mercaptan

HCID 57040155N-propylthiophthalimide

Product 1

HCID 20306439Propyl-thenyl-disulphide

Procedure

Starting from thenylmercaptan and N-propylthiophthalimide there is obtained propyl-thenyl-disulphide. IR (liq.): bands inter alia at 2990, 1455, 1220, 1030, 850, 700 cm-1.

Sources & evidence

ORD record: ord-0a2597b9267849e3990afa2e7c7d57e3
Source dataset: uspto-grants-1980_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04237290

Reaction notes

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