HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → Adipic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | Methyl adipate | HCID 6994472 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Product | Adipic Acid | HCID 196 | — |
Reaction Steps
The electrolytic condensation was conducted in the same manner as described in Example 2 except for changing the neutral salt group from sodium methylate to sodium bicarbonate by using monomethyl adipate obtained by the half esterification of adipic acid. Electrolytic cell voltage was 7.8 volts. Current efficiency was 67.0% and material yield was 79.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237317 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-c749cb49cfde458e975d27a2d42ae542 |
| Source note | uspto-grants-1980_12 |