Phenol → HCID 53433129, compound

HRID 1732539Notes

Reaction equation

HRID 1732539 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Si:8](Cl)(Cl)(Cl)[Cl:9]>>[Cl:9][Si:8].[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 996PhenolHCID 24816Silicon tetrachloride

Product 1

HCID 53433129HCID 53433129, compound

Procedure

About 0.5 mol of fine granular hydrated silica, 0.5 mol of phenol and 1 mol of silicon tetrachloride are slowly added simultaneously while agitating and keeping the temperature below the boiling temperature of the mixture for 1 to 2 hours; the reaction is complete in 2 to 8 hours, thereby producing a phenol chlorosilicon acid resinous product. To this resinous product 1.5 mols of an amino compound, ethylene diamine, are slowly added while agitating for 1 to 2 hours, thereby producing white granules of organic silicon acid resinous product.

Workup

  1. customfor 1 to 2 hours

Sources & evidence

ORD record
ord-78d191eaa3744aff84a20ff1d48dec13
Source dataset
uspto-grants-1980_12
Patent number
US04238375

Reaction notes

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