Sodium borohydride → HCID 70514666, compound

HRID 1732594Notes

Reaction equation

HRID 1732594 reaction equation
[C:1]([N:4]1[C:12]2[C:11]([Cl:13])=[CH:10][CH:9]=[C:8]3[C:14](=[O:22])[CH:15]([NH:17][C:18](=[O:21])[CH2:19][Cl:20])[CH2:16][C:6]([C:7]=23)=[CH:5]1)(=[O:3])[CH3:2].[BH4-].[Na+]>C(O)C>[C:1]([N:4]1[C:12]2[C:11]([Cl:13])=[CH:10][CH:9]=[C:8]3[C@@H:14]([OH:22])[C@H:15]([NH:17][C:18](=[O:21])[CH2:19][Cl:20])[CH2:16][C:6]([C:7]=23)=[CH:5]1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 4311764Sodium borohydrideHCID 20303923HCID 20303923, compound

Product 1

HCID 70514666HCID 70514666, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

An ice cold, solution of 1-acetyl-4-chloroacetamido-8-chloro-3,4-dihydrobenz[cd]indol-5-(1H)-one in ethanol is reduced with excess sodium borohydride to the subject alcohol.

Sources & evidence

ORD record
ord-fb75c191682f4d58b598e6f60ed26ac0
Source dataset
uspto-grants-1980_12
Patent number
US04238486

Reaction notes

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