Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12470613 | HCID 12470613 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20304079 | HCID 20304079 | 97% |
Reaction Steps
76 g (0.286 mol) of 4-cyclohexylphenylphenylcarbinol are introduced in portions into a mixture of 143 ml (2 mols) of thionyl chloride and 200 ml of benzene at 70° C. The reaction mixture is heated to 70° C. for 15 hours and then evaporated. The oil which remains is stirred with petroleum ether, whereupon it solidifies to a crystal sludge. 79 g (96% of theory) of 4-cyclohexylphenyl-phenylchloromethane of melting point 75° C. are obtained. ##STR7##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04238498 |
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| Source dataset | uspto-grants-1980_12 |
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| ORD ID | ord-cc6489ae926a45a1a6cd8b9ef800233f |
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| Source note | uspto-grants-1980_12 |
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