5-Chloro-2-methoxybenzoyl chloride → HCID 17341531, compound

HRID 1732654Notes

Reaction equation

HRID 1732654 reaction equation
Cl.[NH2:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][C:11]([O:13]CC)=[O:12])=[CH:5][CH:4]=1.[Cl:16][C:17]1[CH:18]=[CH:19][C:20]([O:26][CH3:27])=[C:21]([CH:25]=1)[C:22](Cl)=[O:23]>>[Cl:16][C:17]1[CH:18]=[CH:19][C:20]([O:26][CH3:27])=[C:21]([CH:25]=1)[C:22]([NH:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][C:11]([OH:13])=[O:12])=[CH:7][CH:8]=1)=[O:23]

Participants

3

Reactant 2

HCID 123841765-Chloro-2-methoxybenzoyl chlorideHCID 2030435461630-01-1

Product 1

HCID 17341531HCID 17341531, compound

Procedure

By the reaction of ethyl β-(4-aminophenyl)-propionate hydrochloride with 5-chloro-2-methoxybenzoyl chloride. there is obtained β-[4-(5-chloro-2-methoxybenzamido)-phenyl]-propionic acid; m.p. 188°-190° C., after recrystallization from ethanol.

Sources & evidence

ORD record
ord-3034195231d14e15b51406137348226a
Source dataset
uspto-grants-1980_12
Patent number
US04238506

Reaction notes

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