HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidone hydrochloride → HCID 20304748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidone hydrochloride | HCID 3084851 | — |
| Reactant | HCID 17900740 | HCID 17900740 | — |
| Reactant | HCID 20304715 | HCID 20304715 | — |
| Product | HCID 20304748 | HCID 20304748 | — |
Reaction Steps
According to the procedure described in Example 1, the appropriate benzoxazepine is converted to 1-amino-1,2,3,5-tetrahydro-5-methyl-4,1-benzoxazepine hydrochloride, m.p. 198°-200°, which is reacted with 4-piperidone hydrochloride to yield the title compound, m.p. 285°-286° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04238607 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-70023978801a4bd6925209d172b33233 |
| Source note | uspto-grants-1980_12 |