1-Methyl-4-piperidone → HCID 20304650, compound
Reaction equation
[ClH:1].N[N:3]1[C:8]2[CH:9]=[CH:10][C:11]([CH3:13])=[CH:12][C:7]=2[O:6][CH2:5][CH2:4]1.[CH3:14][N:15]1[CH2:20][CH2:19][C:18](=O)[CH2:17][CH2:16]1>>[ClH:1].[CH3:13][C:11]1[CH:10]=[C:9]2[C:8]3[N:3]([C:18]4[CH2:19][CH2:20][N:15]([CH3:14])[CH2:16][C:17]=42)[CH2:4][CH2:5][O:6][C:7]=3[CH:12]=1Participants
3
Procedure
4-Amino-3,4-dihydro-7-methyl-2H-1,4-benzoxazine hydrochloride is reacted with 1-methyl-4-piperidone according to the procedure of Example 110 to yield the title compound, m.p. 248°-249°.
Sources & evidence
- ORD record
- ord-01c3f56b59954db18d36fec5de23f941
- Source dataset
- uspto-grants-1980_12
- Patent number
- US04238607
Reaction notes
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