HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (-)- → HCID 22803897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Reactant | HCID 70582708 | HCID 70582708 | — |
| Product | HCID 22803897 | HCID 22803897 | — |
Reaction Steps
This alcohol was resolved, as in the previous examples, by conversion to the half ester XXXIc and then to the salt with L-(-)-α-methylbenzylamine. Three recrystallizations of this salt from 2-propanol gave 37 g, mp 144°-145° C., αD =+36.0 (c 2.0, CH3OH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04238623 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-fc835117072349b597f62f62b5b7fe76 |
| Source note | uspto-grants-1980_12 |