HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-Butylmercaptoaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | o-Nitrobenzenethiol | HCID 21002 | — |
| Reactant | 2-Pyrrolidinone, 1-(hydroxymethyl)- | HCID 84911 | — |
| Product | 2-Butylmercaptoaniline | HCID 10329960 | — |
Reaction Steps
2-Butylmercaptoaniline was prepared from -2-nitrothiophenol by a two-step reaction sequence consisting of alkylation followed by reduction corresponding to the procedure described in Example 4. The aniline then was condensed with N-methylolpyrrolidone, followed by reaction with chloroacetyl chloride to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239688 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-9bb7ea5ee3214d5ca67c785aa455bc90 |
| Source note | uspto-grants-1980_12 |