Ethyl Bromide → N-Ethyl-N-methyl-2-thiophene methanamine

Beteiligte Stoffe

Reaktionsschritte

Bromoethane (150 ml), triethylamine (7.3 ml) and N-methyl-2-thiophenemethanamine (21.2 g) were stirred at room temperature in toluene (212 ml) for 4 days. The solution was diluted with water, saturated with sodium bicarbonate and extracted with ethyl acetate. The organic extracts were distilled to give the title compound as an oil (13.6 g) b.p. 46° (16 mm).

Herkunft & Nachweise