HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70597144, compound → HCID 70595412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70597144 | HCID 70597144 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70595412 | HCID 70595412 | — |
Reaction Steps
A solution of 2.79 g of 1-isobutylideneamino-3-p-biphenylyl-butane (obtainable by boiling 3-p-biphenylylbutylamine with isobutyraldehyde in benzene for 5 hours) in 75 ml of methanol is hydrogenated, after adding 0.3 g of PtO2, at 20° and normal pressure until hydrogen absorption ceases. The mixture is filtered and worked up in the customary manner to give 1-isobutylamino-3-p-biphenylyl-butane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239759 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-a2495812bc904829aae3919b8d438dd6 |
| Source note | uspto-grants-1980_12 |