HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 54571361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20302325 | HCID 20302325 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54571361 | HCID 54571361 | — |
Reaction Steps
25.9 g of 3-(4'-fluoro-4-biphenylyl)-3-hydroxybutylamine p-toluenesulfonate are boiled with 1 g of p-toluenesulfonic acid in 500 ml of toluene for 2 hours under a water separator, and the mixture is cooled and worked up with sodium hydroxide solution to give 3-(4'-fluoro-4-biphenylyl)-2-buten-1-yl-amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239759 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-e6d26dab110d4c8ca74802f083c7fa32 |
| Source note | uspto-grants-1980_12 |