Formaldehyde → HCID 70595239, compound

HRID 1733058Notes

Reaction equation

HRID 1733058 reaction equation
[CH:1]([NH:4][CH2:5][CH2:6][CH:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[CH3:8])([CH3:3])[CH3:2].[CH2:21]=O>C(O)=O>[CH3:21][N:4]([CH2:5][CH2:6][CH:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[CH3:8])[CH:1]([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 712FormaldehydeHCID 70595162HCID 70595162, compound

Product 1

HCID 70595239HCID 70595239, compound

Reagents, catalysts & solvents 1

HCID 284Formic AcidSolvent

Procedure

A mixture of 2.67 g of 1-isopropylamino-3-p-biphenylylbutane, 12 ml of formic acid and 2 g of 40% formaldehyde solution is heated at 60° for 3 hours and then at 100° for 12 hours and is then evaporated. 1-(N-Methyl-N-isopropylamino)3-p-biphenylyl-butane is obtained after working up in the customary manner.

Workup

  1. temperatureis heated at 60° for 3 hours
  2. customis then evaporated

Sources & evidence

ORD record
ord-75b7af8adac8446485c33c873209415b
Source dataset
uspto-grants-1980_12
Patent number
US04239759

Reaction notes

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