Benzene → HCID 86735981, compound

HRID 1733060Notes

Reaction equation

HRID 1733060 reaction equation
[C:1]1([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH:7]([CH3:11])[CH2:8][CH2:9][NH2:10].C1C=CC=CC=1.[C:24](OC(=O)C)(=[O:26])[CH3:25]>N1C=CC=CC=1>[C:24]([NH:10][CH2:9][CH2:8][CH:7]([C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:1]=1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH3:11])(=[O:26])[CH3:25]

Participants

5

Reactant 3

HCID 241BenzeneHCID 7918Acetic AnhydrideHCID 70595812HCID 70595812, compound

Product 1

HCID 86735981HCID 86735981, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A mixture of 2.25 g of 3-p-biphenylyl-butylamine, 20 ml of benzene, 1 ml of pyridine and 1 ml of acetic anhydride is stirred for 3 hours at 25°. 1-Acetamido-3-p-biphenylylbutane is obtained after working up in the customary manner.

Sources & evidence

ORD record
ord-373a0768d78b49e4b7bdccce1680850f
Source dataset
uspto-grants-1980_12
Patent number
US04239759

Reaction notes

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