HRID1733359

反应详情

EQUATION

反应方程式

HRID 1733359 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4.65 gm of 4-hydroxy-2-methylmercapto-5-nitropyrimidine (0.025 mol) are dissolved with heating in 150 ml of ethanol and refluxed for 5 hours with 4.68 gm of aniline (0.05 mol). The precipitated product is extracted in the cold, washed with ethanol and dried.

WORKUP

后处理

  1. extractionThe precipitated product is extracted in the cold
  2. washwashed with ethanol
  3. customdried