Aniline → HCID 178526816, compound

HRID 1733359Notes

Reaction equation

HRID 1733359 reaction equation
[OH:1][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][N:5]=[C:4](SC)[N:3]=1.[NH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>C(O)C>[NH:13]([C:4]1[N:3]=[C:2]([OH:1])[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][N:5]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

4

Reactant 2

HCID 6115AnilineHCID 178503473C5H5N3O3S

Product 1

HCID 178526816HCID 178526816, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

4.65 gm of 4-hydroxy-2-methylmercapto-5-nitropyrimidine (0.025 mol) are dissolved with heating in 150 ml of ethanol and refluxed for 5 hours with 4.68 gm of aniline (0.05 mol). The precipitated product is extracted in the cold, washed with ethanol and dried.

Workup

  1. extractionThe precipitated product is extracted in the cold
  2. washwashed with ethanol
  3. customdried

Sources & evidence

ORD record
ord-bee777dbd30a44bd92fc4b9edb4b28f5
Source dataset
uspto-grants-1980_12
Patent number
US04241056

Reaction notes

Loading…