HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1,2-Benzisothiazolin-3-one manganese(II)chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzisothiazole | HCID 9225 | — |
| Reactant | Manganese(2+) dichloride | HCID 10313134 | — |
| Product | 1,2-Benzisothiazolin-3-one manganese(II)chloride | HCID 70534353 | 77% |
Reaction Steps
To a solution of 1.26 g (0.01 mol) of anhydrous manganese chloride was added 4.5 g (0.03 mol) of 1,2-benzisothiazolin in 30 ml of water. The solution was concentrated to give a tan colored solid. The solid was thoroughly washed with dry acetone, filtered and dried at room temperature to yield 3.47 g (77%) of product, m.p.>250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04241214 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-c68064862bc44f228505eea6ecf7f486 |
| Source note | uspto-grants-1980_12 |