Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Dichloro(hexyl)silane | HCID 92038703 | — |
| Catalyst | HCID 178420539 | HCID 178420539 | — |
| Product | n-Hexylphenethyldichlorosilane | HCID 20299100 | 91.1% |
Reaction Steps
3.80 g (20.5 millimol) of n-hexyldichlorosilane, 2.00 g (19.2 millimol) of styrene, and 0.023 g (1.92×10-5 mol) of tetrakis(triphenylphosphine)platinum (O) were introduced into a flask and reacted with stirring by heating in an oil bath at 60° C. for 8 hours and then subjected to distillation under a reduced pressure to produce 5.6 g (17.5 millimol) of n-hexylphenethyldichlorosilane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04242272 |
|---|
| Source dataset | uspto-grants-1980_12 |
|---|
| ORD ID | ord-4683dd3e1a49444ebbe1ea160db91666 |
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| Source note | uspto-grants-1980_12 |
|---|
