HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → Monophenethyldichlorosilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Dichlorosilane | HCID 61330 | — |
| Catalyst | Chlorotris(triphenylphosphine)rhodium(I) | HCID 84599 | — |
| Product | Monophenethyldichlorosilane | HCID 123907249 | 99.2% |
Reaction Steps
73.2 g (725 millimol) of dichlorosilane, and 92.7 g (890 millimol) of styrene were reacted in the presence of 0.1164 g (1.68×10-4 mol) of chlorotris(triphenylphosphine)rhodium (I) as in example 3 at 100° C. for 16 hours and then the reacted liquid was distilled to obtain 147.6 g of monophenethyldichlorosilane (b.p. 95° C./7 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04242272 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-0d6cb52baa0949239febb8bb91339b59 |
| Source note | uspto-grants-1980_12 |