HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzonitrile → HCID 53676860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzonitrile | HCID 13396 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 53676860 | HCID 53676860 | — |
Reaction Steps
A mixture of 39 g (0.33 m) of 4-aminobenzonitrile and 250 ml of POCl3 was heated under reflux for 3 hours. The excess POCl3 was removed by vacuum distillation to yield 72.7 g, m.p. softens 128°, melts 131°-133.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04242325 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-1e31659ad8724260bbfcafb78b4bbcd8 |
| Source note | uspto-grants-1980_12 |