Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Sulfanilic acid | HCID 8479 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20437337 | HCID 20437337 | — |
| Product | HCID 23673789 | HCID 23673789 | — |
Reaction Steps
A methylene chloride solution of N-trifluoroacetyl-4-(hexadecylamino)benzoyl chloride (4.8 g.) is added to a solution of 1.8 g. of sulfanilic acid in 1 N sodium hydroxide at 0° C. After 3 hours, the solution is warmed to 60° C. briefly and the whole evaporated to dryness. The residue is extracted with a small amount of cold water and the resulting white solid crystallized from aqueous ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04242273 |
|---|
| Source dataset | uspto-grants-1980_12 |
|---|
| ORD ID | ord-e01b8509e2754d79a8b41b826dbe334e |
|---|
| Source note | uspto-grants-1980_12 |
|---|
