HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetamide → HCID 20300116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 53868-37-4 | HCID 54170778 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20300116 | HCID 20300116 | — |
Reaction Steps
In the manner described in Example 6, a solution of 13.7 g. of sodium methoxide and 10.7 g. of cyanoacetamide in 250 ml. of methanol and 24.0 g. of 3-(dimethylamino)-2-(3-methylphenyl)-2-propenal is refluxed overnight to give 12.0 g. of the product of the Example as a yellow solid, m.p. 254.5°-260° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04242515 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-d1c2d92976b349c883d8c730455c818f |
| Source note | uspto-grants-1980_12 |