HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 10737101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 1-(Triphenylphosphoranylidene)acetone | HCID 15038 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10737101 | HCID 10737101 | — |
Reaction Steps
By reaction of 15.0 g of methylcarbonylmethylenetriphenyl phosphorane in 471 ml of tetrahydrofuran with 31.0 ml of butyllithium and 4.28 ml of allyl bromide analogously to 7, the title compound is obtained as crystallized oil with a melting point of 92°-93° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532228 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-01443230ed95495ca3719c3c76ac4032 |
| Source note | uspto-grants-1996_07 |