HRID1733923

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID321974

6-bromohexanamide

C6H12BrNO

HCID15837955

未命名化合物

PRODUCTS

生成物

结构：NC(=O)CCCC1(Cc2ccncc2)c2ccccc2-c2ccccc21.NC(=O)CCCC1(Cc2ccncc2)c2ccccc2-c2ccccc21.O

HCID70279811

未命名化合物

收率 100%

PROCEDURE

实验过程

By substituting 4-bromobutyl acetamide and 9-(4-pyridinylmethyl)-9H-fluorene in Ex. 1, the product was obtained in 100% yield; mp 50°-52° C.

WORKUP

后处理

custom1, the product was obtained in 100% yield

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-677d44f7b57d45f28d80c10a23d01315
来源数据集: uspto-grants-1996_07
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05532249
来源说明: uspto-grants-1996_07

反应 SMILES

BrCC[CH2:4][CH2:5][CH2:6][C:7]([NH2:9])=[O:8].[N:10]1[CH:15]=[CH:14][C:13]([CH2:16][CH:17]2[C:29]3[CH:28]=[CH:27][CH:26]=[CH:25][C:24]=3[C:23]3[C:18]2=[CH:19][CH:20]=[CH:21][CH:22]=3)=[CH:12][CH:11]=1>>[OH2:8].[N:10]1[CH:11]=[CH:12][C:13]([CH2:16][C:17]2([CH2:4][CH2:5][CH2:6][C:7]([NH2:9])=[O:8])[C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][C:23]=3[C:24]3[C:29]2=[CH:28][CH:27]=[CH:26][CH:25]=3)=[CH:14][CH:15]=1.[N:10]1[CH:11]=[CH:12][C:13]([CH2:16][C:17]2([CH2:4][CH2:5][CH2:6][C:7]([NH2:9])=[O:8])[C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][C:23]=3[C:24]3[C:29]2=[CH:28][CH:27]=[CH:26][CH:25]=3)=[CH:14][CH:15]=1