HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12793231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Chloro-5-(methylsulfanyl)benzoic acid | HCID 608814 | — |
| Product | HCID 12793231 | HCID 12793231 | — |
Reaction Steps
A mixture of 2.03 g of 2-chloro-5-(methylthio)benzoic acid and 10 ml of thionyl chloride is heated on a steam bath for 1 hour. The volatiles are removed under vacuum and 20 ml of toluene added and removed under vacuum (2 times) to give 2.2 g of brown needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532235 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-9a34ff18079942d8856d388835df36e3 |
| Source note | uspto-grants-1996_07 |