HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → 4-(2-Phenylbenzoylamino)-benzoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-[(2-phenylbenzoyl)amino]benzoic Acid | HCID 10543502 | — |
| Product | 4-(2-Phenylbenzoylamino)-benzoylchloride | HCID 11450501 | — |
Reaction Steps
A mixture of 1.39 g of 4-[([1,1'-biphenyl]-2-carbonyl)amino]benzoic acid in 2.0 ml of thionyl chloride is heated on a steam bath for 1 hour. Cold hexane is added and the crystalline solid collected and dried to give 1.34 g of the desired product, m.p. 118°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532235 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-066c92f39bbe46bfb4967ba72b9a2425 |
| Source note | uspto-grants-1996_07 |